3-Bromo phenyl methyl

Name	3-Bromophenyl methyl sulfone
Synonyms	3-BROMOPHENYLMETHYLS 3-Bromo phenyl methyl 3-BROMOPHENYLMETHYLSULFONE 3-Bromophenyl methyl sulfone 3-Bromo phenyl methyl sulfone 1-bromo-3-(methylsulfonyl)benzene 1-Bromo-3-methanesulfonyl-benzene Benzene,1-bromo-3-(methylsulfonyl)-
CAS	34896-80-5
EINECS	639-429-9
InChI	InChI=1/C7H7BrO2S/c1-11(9,10)7-4-2-3-6(8)5-7/h2-5H,1H3

Molecular Formula	C7H7BrO2S
Molar Mass	235.1
Density	1.595±0.06 g/cm3(Predicted)
Melting Point	100-104°C
Boling Point	362.8±34.0 °C(Predicted)
Flash Point	173.2°C
Solubility	Chloroform
Vapor Presure	3.93E-05mmHg at 25°C
Appearance	Solid
Color	White
Storage Condition	Sealed in dry,Room Temperature
Refractive Index	1.563
MDL	MFCD03095326

Safety Description	24/25 - Avoid contact with skin and eyes.
HS Code	29309090

Introduction	3-bromophenyl methyl sulfone is an organic intermediate, which can be obtained by oxidation of 3-bromthioanisole. There are reports that it can be used to prepare mTOR inhibitors.
Uses	3-bromophenyl methyl sulfone is a hydrocarbon organic substance and can be used as a pharmaceutical intermediate.
preparation	3-bromothioanisole (8.7g, 43mmol) was added to dichloromethane (125 ml) and cooled to 0 ℃. To which 3-chloroperbenzoic acid (22.2g, 129mmol) was added. m- CPBA is not completely dissolved. Stir the reaction mixture overnight. The reaction was quenched with saturated thiosulfuric acid sodium (150 ml) solution. The product was extracted with EtOAc(3 × 100 ml). Combine the organic distillate parts, wash with salt water (75 ml), and dry with sodium sulfate. The organic liquid was then concentrated to give 9.89 grams (97%) of 3-bromophenylmethyl sulfone.

Last Update：2024-04-09 19:05:05

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